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Instrument

ASAP 2020 Plus - Physisorption

 

 

Advanced Capabilities through Optional Configurations. The ASAP 2020 Plus can be configured to your specific needs with the option of upgrading at a later date as your analytical requirements change, maximizing the utility of this instrument and your investment. Choose from low surface area, to heated vapor, to micropore capability. Add a cryostat, an external detector, or configure the unit for enhanced chemical resistance when working with aggressive vapors.

The ASAP 2020 Plus permits one instrument to accommodate almost any surface characterization need in your lab. Unique and Innovative Isothermal Jacket Cold Zone Control Isothermal jackets are guaranteed for the life of the instrument and ensure a constant thermal profile along the full length of both the sample and saturation pressure tubes.

  • Subambient Temperature Controllers Brochure



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  • Part No. 202-50217-00

    ASAP 2020 Plus Automatic Micropore Physisorption Analyzer

    High-performance physical sorption analyzer producing research grade analytical measurements for determining specific surface area and pore size distribution from 3.5 to 5000 Angstroms. Features continuous saturation pressure measurement capability. Includes MicroActive interactive data reduction software which provides improved control interface, real-time performance indicators, and preventive maintenance scheduling information.  Oil-free high vacuum system for analysis and separate oil-free high vacuum system for degas reduce maintenance costs and eliminate any potential of system contamination from oil filled vacuum pumps.
    Analysis Gases:
    N2, O2, Ar, Kr, CO2, CO, H2, Butane or any non-corrosive gases

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    Part No. 202-50103-00
    ASAP 2020 Plus Automatic High Vacuum Physisorption Analyzer
    High-performance physical sorption analyzer producing research grade analytical measurements for determining specific surface area and pore size distribution from 17 to 5000 Angstroms. Features continuous saturation pressure measurement capability. Includes MicroActive interactive data reduction software which provides improved control interface, real-time performance indicators, and preventive maintenance scheduling information.  Oil-free high vacuum system for analysis and separate oil-free high vacuum system for degas reduce maintenance costs and eliminate any potential of system contamination from oil filled vacuum pumps. 10-Torr transducer in analysis manifold for low surface area measurements using Krypton.
    Analysis Gases:N2, O2, Ar, Kr, CO2, CO, H2, Butane or any non-corrosive gases
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    Part No. 202-50227-00
    ASAP 2020 Plus Automatic Micropore Physisorption Analyzer with Kalrez™
    High-performance physical sorption analyzer producing research grade analytical measurements for determining specific surface area and pore size distribution from 3.5 to 5000 Angstroms. Features continuous saturation pressure measurement capability. Includes MicroActive interactive data reduction software which provides improved control interface, real-time performance indicators, and preventive maintenance scheduling information.  Oil-free high vacuum system for analysis and separate oil-free high vacuum system for degas reduce maintenance costs and eliminate any potential of system contamination from oil filled vacuum pumps.This unit includes a manifold designed to permit use of unsaturated hydrocarbons. Uses Kalrez™ sealing materials necessary for analyses with unsaturated hydrocarbons such as benzene, toluene and other adsorbates.
    Analysis Gases:
    N2, O2, Ar, Kr, CO2, CO, H2, Butane or any non-corrosive gases as well as unsaturated hydrocarbons
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    Part No. 202-50000-11
    ASAP 2020 PLUS N, 110 V
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    Part No. 202-50000-22
    ASAP 2020 PLUS N, 230V
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    Part No. 202-50100-00
    ASAP 2020 PLUS N, DRY
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    Accessories

    Analyzer Optional Equipment

    Part No. 025-00202-00
    Chiller Dewar Option, permits connection of a recirculating bath to a closed plumbing system which is situated inside of a dewar in order to control analyses at a variety of temperatures.
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    Part No. 021-00000-00

    Model 021 LN2 transfer system, for easy filling of sample dewars;includes 44 L dewar, mobile platform, and pump with 100 cm discharge line. More information »

     

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    Part No. 025-26004-00
    Recirculating Bath, -28 °C TO 200 °C, 115V 60Hz, Refrigerated and Heating Circulator for temperature control of the Chiller Dewar.
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    Part No. 025-33001-00
    RTD Probe for Recirculating Bath Temperature Control, Optional RTD mounted in the bath and connected to the controller on the recirculating bath for more accurate temperature control. (for use with 025/26004/00)
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    Part No. 205-33005-00
    ISO Controller Temperature Control Device. A Peltier technique based temperature controller designed to maintain a constant temperature between 0 °C and 80 °C. Replaces analysis Dewar
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    Analyzer Add-on Options and Upgrades

    Part No. 202-33055-00
    Vapor Option, Field Installation, must be installed by a Micromeritics trained service technician, and instrument must undergo a Micromeritics service review prior to installation.
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    Part No. 202-33057-00
    Vacuum Cold Trap Option, must be installed by a Micromeritics trained service technician, and instrument must undergo a Micromeritics service review prior to installation.
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    Part No. 202-33611-00
    Nitrogen to Multigas Upgrade, adds 10 mmHg transducer and high vacuum pump, must be installed by a Micromeritics trained service technician, and instrument must undergo a Micromeritics service review prior to installation.
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    Part No. 202-33612-00
    Multigas to Micropore Upgrade, adds 0.1 mmHg transducer, supplied with micropore reference material, must be installed by a Micromeritics trained service technician, and instrument must undergo a Micromeritics service review prior to installation.
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    Part No. 202-33613-00
    Chemisorption Upgrade, upgrades a physisorption only instrument to a chemisorption instrument, must be installed by a Micromeritics trained service technician, and instrument must undergo a Micromeritics service review prior to installation.
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    Cables

    Part No. 003-63801-01
    Cable, Ethernet straight-thru
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    Dewar and Accessories

    Part No. 202-25849-00
    Dewar, 3 liter, cold trap
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    Part No. 202-25850-00
    Dewar, 3 liter, analysis
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    Part No. 202-31707-00
    Dewar cover, analysis
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    Part No. 202-31708-00
    Dewar cover, cold trap
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    Part No. 202-33053-00
    Stainless Steel Dewar Kit, 4 liter, wide mouth, includes analysis dewar, cold trap dewar, and elevator adapter. Typically provides greater than 40 hours of unattended analysis.
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    Part No. 240-25901-00
    Dewar depth gauge
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    Gas Cylinder Accessories and Replacement Parts

    Part No. 004-25103-00
    Ferrule, front, teflon 1/4 in., for use with 1/8 in. tube × 1/4 in. tube reducer
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    Part No. 004-25104-00
    Ferrule, rear, nylon 1/4 in., for use with 1/8 in. tube × 1/4 in. tube reducer
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    Part No. 004-25549-00
    Reducer, 1/8 in tube × 1/4 in. tube, brass, accepts 1/8 in. tube, connects to 1/4 in. swage fittings
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    Part No. 004-25913-00
    1/8 Peek Ferrule Set for sealing gas inlet lines into the gas inlet manifold assemblies
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    Part No. 004-33601-00
    Expansion Kit, adds an additional outlet to the gas regulator, includes fittings and instructions
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    Part No. 004-33601-00
    Expansion Kit, adds an additional outlet to the gas regulator, includes fittings and instructions
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    Part No. 004-33602-00
    Pressure Relief Kit, prevents excessive gas pressure in the event of regulator failure (not to be used with toxic gases)
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    Part No. 004-62230-32
    Gas pressure regulator, CGA 320 fitting (CO²), 30 psig
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    Part No. 004-62230-35
    Gas pressure regulator, CGA 350 fitting (CO, H²), 30 psig
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    Part No. 004-62230-54
    Gas pressure regulator, CGA 540 fitting (O²), 30 psig
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    Part No. 004-62230-58
    Gas pressure regulator, CGA 580 fitting, 30 psig (He, N², Kr, Ar)
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    Part No. 004-62230-326
    Gas pressure regulator, CGA 326 fitting (N²O), 30 psig
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    Part No. 004-62230-705
    Gas pressure regulator, CGA 705 fitting (NH³), 30 psig
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    Part No. 201-25818-00
    Gas Inlet Line, 6 ft, SS
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    Part No. 201-25818-01
    Gas Inlet Line, 16 ft (5 m), SS
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    Part No. 290-25846-00
    Gas Inlet Line, 1/8 in × 6 ft, copper
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    Part No. 290-25846-01
    Gas Inlet Line, 1/8 in × 16 ft (5 m), copper
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    Heating Mantle

    Part No. 003-26043-00
    Heating mantle with type K thermocouple, 450 °C maximum, 24 V
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    Part No. 003-26045-00
    Heating mantle with type K thermocouple, 450 °C maximum, 24 V, side-laced to accommodate monolithic & nonstandard sample tubes
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    Part No. 230-25808-00
    Heating mantle clip
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    Operating Supplies and Replacement Parts

    Part No. 004-25006-00
    O-ring, size 006, Buna-N, for P° tube
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    Part No. 004-25466-00
    O-ring, -010 70 Durometer Buna-N, for sealing frit in sample tube port
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    Part No. 004-25673-00
    O-ring, size 008, Kalrez for exhaust port filter
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    Part No. 004-25674-00
    O-ring, -006 Kalrez 7075, for replacement on the Kalrez inlet manifold assembly
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    Part No. 004-27041-00
    Frit, µm SS 1/4D × 1/16T, for replacement in sample tube port
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    Part No. 004-27056-00
    Exhaust filter, 20 µm, 3/16 in. diameter
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    Part No. 004-54130-00
    Removal tool for CheckSeal opener
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    Part No. 200-25840-00
    Saturation pressure tube, includes isothermal jacket
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    Part No. 206-14701-00
    Dewar shield, for use on sample port, cold trap, and degas ports
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    Part No. 202-14702-00
    Dewar shield, for use with Chiller Dewar Option
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    Part No. 202-33010-06
    Kalrez operating supplies (6 month supply), Kel-F gaskets for manifold valves, Kalrez O-rings, Kalrez valve seat plunger
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    Part No. 202-33010-12
    Kalrez operating supplies (6 month supply), Kel-F gaskets for manifold valves, Kalrez O-rings, Kalrez valve seat plunger, spring for Kalrez plungers, Chemraz inert valve
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    Part No. 202-33100-06
    Physisorption operating supplies (6 month supply), O-rings, sample port frits, 1/8 Peek ferrule sets, sample tubes
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    Part No. 202-33100-12
    Physisorption operating supplies (12 month supply), O-rings, sample port frits, 1/8 Peek ferrule sets, sample tubes, filler rods, sample tube brush, isothermal jacket, dewar cover, sample tube stoppers
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    Reference Material

    Part No. 004-16816-00
    Reference material, low surface area (krypton)
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    Part No. 004-16821-00
    Reference material, high surface area
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    Part No. 004-16843-00
    Reference material, micropore, 13X
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    Part No. 004-16844-00
    Reference material, micropore, Y-zeolite
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    Sample Tube Accessories

    Part No. 004-54609-00
    Brush for cleaning sample tube
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    Part No. 004-54618-00
    Tool, for removing sample port O-ring
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    Part No. 202-33052-00
    22 mm ID Sample Tube Kit (see table for kit contents)
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    Part No. 240-14855-00
    Sample tube rack
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    Part No. 240-25853-00
    Sample tube funnel
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    Part No. 240-32805-00
    Sample tube support, assists sample weighing
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    Software and Manuals

    Part No. 202-20828-00
    ASAP 2020 Plus Physisorption software program
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    Part No. 202-33027-00
    MicroActive Software Package, interactive data analysis software
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    Part No. 202-42800-00
    ASAP 2020 Plus Operator Manual (includes binder and dividers)
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    Vacuum Pump and Accessories

    Part No. 004-16003-01
    Vacuum pump oil, 1 liter
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    Part No. 004-16830-00
    Activated alumina, 500 grams, for oil vapor trap
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    Part No. 004-25652-00
    O-ring, size 217, for oil vapor trap
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    Part No. 004-27040-00
    Vacuum pump exhaust filter
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    Part No. 004-32177-00
    Funnel, for filling vacuum pump with oil
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    Part No. 004-62023-01
    Service kit, for Vaccubrand dry forepump
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    Part No. 062-00200-00
    Vacuum forepump, dry, for systems with high-vacuum option, 115/230 VAC
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    Part No. 062-33002-00
    Activated alumina oil vapor trap, for one vacuum pump
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    Part No. 062-62801-23
    VAC (replacement pump only, does not include exhaust filter, foreline trap, or vacuum pump tray)
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    Part No. 062-62801-11
    VAC (replacement pump only, does not include exhaust filter, foreline trap, or vacuum pump tray)
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    Valves

    Part No. 003-22633-00
    Valve, for Kalrez gas inlet manifold
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    Part No. 004-25459-00
    Valve plunger, Kalrez seal, for analysis manifold
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    Part No. 004-25936-00
    Valve spring, for Kalrez plunger
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    Part No. 201-22600-00
    Valve spring, for Buna-N plunger, for analysis manifold
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    Part No. 250-25608-00
    Valve gasket, Kel-F, for analysis manifold
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    Part No. 250-25627-00
    Valve plunger, Buna-N seal, for analysis manifold
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    Vapor Adsorption Accessories and Replacement Parts

    Part No. 003-20656-02
    Cable, M/M 15 Pin D 5 ft straight-thru, for connecting the controller to the vapor source
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    Part No. 003-20656-03
    Cable, M/M 25 Pin D 5 ft straight-thru, for connecting the controller to the manifold
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    Part No. 004-25031-00
    O-ring, -110 Kalrez 7075 .362 ID, for replacement on the Vapor Stem Assembly
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    Part No. 004-25103-00
    Ferrule,front, 1/4 in. teflon, for sealing the vapor stem assembly to the vapor connector
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    Part No. 004-25104-00
    Ferrule, rear, 1/4 in. nylon, for sealing the vapor stem assembly to the vapor connector
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    Part No. 004-25465-00
    O-ring, -010 Kalrez 7075, for replacement on the Vapor Stem Assembly
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    Part No. 004-61004-00
    Dewar flask, 350 ml
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    Part No. 004-61630-00
    Glass vapor tube
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    Part No. 202-25878-00
    Sample port insulator
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    Part No. 202-33054-02
    Sample tube conductor kit, contains 2 sample tube conductors and 2 O-rings
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    Part No. 202-34150-02
    Vapor Stem Assembly
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    Sample Tubes and Components for Physisorption

    1/4 in., 3/8 in., and 1/2 in. Sample Tubes
    Part No. 004-25465-00 - O-ring, size 010, Kalrez, for 1/4 in. sample tube
    A)
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    Part No. 004-25466-00, O-ring, size 010, Buna-N, for 1/4 in. sample tube
    A)
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    Part No. 240-25803-00, Ferrule, 1/4 in.
    B)
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    Part No. 004-32604-00, Cap (stopper) for 1/4 In. sample tube (not shown)
    C)
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    Part No. 202-25901-00, Isothermal jacket, 1/4 in
    D) .
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    Part No. 240-61001-00, Sample tube, 1/4 in.
    E)
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    Part No. 240-61014-00, Volume displacement insert, 1/4 in
    F) .
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    Part No. 004-25022-00, O-ring, size 012, Buna-N, for 3/8 in. sample tube
    G)
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    Part No. 004-25022-01, O-ring, size 012, Kalrez, for 3/8 in. sample tube
    G)
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    Part No. 240-25802-00, Ferrule, 3/8 in.
    H)
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    Part No. 004-32004-00, Stopper, for 3/8 in. sample tubes
    I)
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    Part No. 202-25902-00, Isothermal jacket, 3/8 in
    J)
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    Part No. 240-61002-00, Sample tube, 3/8 in.
    K)
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    Part No. 240-61015-00, Volume displacement insert, 3/8 in
    L)
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    Part No. 260-25891-00, Opener, seal frit, for 1/2 in. sample tube
    M)
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    Part No. 004-25044-00, O-ring, size 013, Buna-N, for 1/2 in. sample tube
    N)
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    Part No. 004-25474-00, O-ring, size 013, Kalrez, for 1/2 in. sample tube
    N)
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    Part No. 260-25843-00, Ferrule, 1/2 in.
    O)
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    Part No. 240-32000-00, Stopper, for 1/2 in. sample tube
    P)
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    Part No. 260-25890-00, Seal Frit with built-in check valve for air-sensitive samples
    Q)
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    Part No. 202-25903-00, Isothermal jacket, 1/2 in. sample tube
    R)
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    Part No. 240-61003-00, Sample tube, 1/2 in.
    S)
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    Part No. 300-25824-00, Nut, sample tube
    U)
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    Part No. 240-61016-00, Volume displacement insert, 1/2 in
    T)
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    Part No. 300-25824-00, Nut, sample tube
    U)
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    Sample Tube Kit - 22 mm

    Part No. 202-33052-00

    Kit Contains:

    Qty. Part Number Description
    10 004-25609-02 O-ring, -022, 70 Buna-N
    5 004-32230-00 Stopper, rubber, for 22 mm ID yube
    1 202-25868-00 Fitting, sample port, 25 mm sample tube
    3 202-25869-00 Nut, for 25 mm sample tube
    3 202-25870-00 Ferrule for 25 mm sample tube
    2 202-25871-00 Fitting, degas port, 25 mm sample tube
    2 202-25904-00 Isothermal jacket, for 25 mm OD sample tube
    1 202-31709-00 Dewar cover, 25 mm OD sample tube
    5 202-61022-00 Sample tube, 22 mm ID, 25 mm OD
    5 202-61022-01 Filler rod for 22 mm ID sample tube
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    Items contained in Sample Tube Kit - 22 mm

    Part No. 004-25609-02
    O-ring, -022, 70 Buna-N
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    Part No. 004-32230-00
    Stopper, rubber, for 22 mm ID tube
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    Part No. 202-25868-00
    Fitting, sample port, 25 mm sample tube
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    Part No. 202-25869-00
    Nut, for 25 mm sample tube
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    Part No. 202-25870-00
    Ferrule for 25 mm sample tube
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    Part No. 202-25871-00
    Fitting, degas port, 25 mm sample tube
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    Part No. 202-25904-00
    Isothermal jacket, for 25 mm OD sample tube
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    Part No. 202-31709-00
    Dewar cover, 25 mm OD sample tube
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    Part No. 202-61022-00
    Sample tube, 22 mm ID, 25 mm OD
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    Part No. 202-61022-01
    Filler rod for 22 mm ID sample tube
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    Chiller Dewar Liquid Recirculation System

    Part No. 025-00202-00
    For ASAP 2020 Plus - A closed plumbing system that circulates fluid from a temperature controlled bath into a small dewar filled with antifreeze in which the sample tubes are immersed
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    Cryostat I Single-Stage Cryogenic Refrigerator Based on the Gifford-McMahon Principle

    The Micromeritics Cryostat I is a closed-cycle cryocooler based on the Gifford-McMahon (GM) refrigeration principle. It uses helium gas from a helium compressor to generate cryogenic temperatures. The refrigeration effect of the GM cooler results from a series of thermodynamic processes acting on the helium gas that includes: charging and compression, displacement and heat exchange with the regenerator, expansion and heat absorption (cooling effect).
    The Cryostat I eliminates the need for liquid nitrogen and can obtain temperatures below the 77 K of liquid nitrogen. The unit is mounted on the Micromeritics instrument with a specially designed fixture. The cold head of the device is positioned at the unit to maintain precise temperature control of the sample tubes. The Cryostat I’s cold head is then connected to a floor mounted compressor.
    Part No. Call Salesrep for info

    Please contact your U.S.A. sales engineer or distributor for a quote on these products.

    Links:

    U.S.A. Sales Engineer Locator »    |    Distributor Locator »

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    Iso Controller Sub-Ambient, Thermoelectric Cooled Dewar

    Micromeritics’ ISO Controller utilizes thermoelectric cooling based on the Peltier principle. The unit is designed to maintain a constant temperature between 0 °C and 80 °C when using CO2, N2, and other gases for adsorption analysis. The device rapidly cools and efficiently maintains temperature with minimal electrical current required. The sample area will accommodate up to 3 sample tubes. Heat removal is uniform and accurate when the unit is used with an appropriate liquid (ambient water or liquid antifreeze). The dewar section is placed on the instrument dewar elevator and then raised into position for analysis.
    Part No. 205-33005-00
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    Chiller Dewar Option Replacement Components

    Part No. 025-25820-00, Hose Assembly
    Hose assembly for connecting the Chiller Dewar to a recirculation bath (2 each required per Chiller Dewar Assembly)
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    Part No. 025-63801-00, Recirculating Bath Temp Control RTD
    Replacement for the RTD cable supplied in the Recirculation Bath Temperature Control RTD Kit
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    Part No. 202-14702-00, Dewar shield
    Dewar shield for use with Chiller Dewar
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    Cold Trap Tubes and Components

    Part No. 004-25469-00
    O-ring, Buna-N, size 014
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    Part No. 004-61063-00
    Tube, 1/2 in. OD stem, cold trap
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    Part No. 200-25979-00
    Nut, cold trap
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      Go