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Instrument

3Flex Surface Characterization Analyzer

Micromeritics 3Flex Surface Characterization Analyzer is a fully automated, three-station instrument capable of high-performance physisorption (mesopore and micropore) and chemisorption analyses with superior accuracy, resolution, and data reduction.  

Each analysis station is upgradeable from mesopore to micropore with the option of designating one station for chemisorption analyses. All analysis stations can be configured for krypton analysis of low surface area materials. Vapor sorption capability is standard. A single 3Flex with its minimal footprint and three configurable analysis stations eliminates costly investment in multiple instruments and additional bench space. The 3Flex is ideally suited for the characterization of MOFs, zeolites, activated carbons, adsorbents, and a wide variety of porous and non-porous materials.

 

 

 

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Part No. 350-00002-00 PHYSISORPTION 1 standard port, 2 micropore ports
PHYSISORPTION 1 standard port, 2 micropore ports
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Part No. 350-00003-00 PHYSISORPTION 3 micropore ports

 

 

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Part No. 350-33602-00 PHYSISORPTION Port Upgrade Kit for Micropore option
Port Upgrade Kit for Micropore option - adds 10 torr and 0.1 torr transducer on each port to be upgraded to micropore capability - This option is service installled.

 

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Part No. 350-33015-00 Vapor Adsorption Option
includes a stainless steel reservoir, isolation valve, and heating mantle. Provides ability to perform three vapor analyses simultaneously.
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Part No. 350-00031-00 CHEMISORPTION Configured with one port for micropore
350-00031-00 CHEMISORPTION Configured with one port for micropore (physisorption) analysis. Analysis Gases: N2, O2, Ar, Kr, CO2, CO, H2, Butane or any non-corrosive gases
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Part No. 350-00032-00 Configured with two ports for micropore
(physisorption) analysis. Analysis Gases: N2, O2, Ar, Kr, CO2, CO, H2, Butane or any non-corrosive gases
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Part No. 350-00033-00 Configured with three ports for micropore
(physisorption) analysis. Analysis Gases: N2, O2, Ar, Kr, CO2, CO, H2, Butane or any non-corrosive gases
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Part No. 350-33640-00 3Flex Chemi-TCD Option
Basic with Software; includes thermal conductivity detectors (TCDs) a septum and a cold trap for analyzing temperature programmed reactions.
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Part No. 350-33641-00 3Flex Chemi-TCD option w/loop valve and restrictor;
includes thermal conductivity detectors (TCDs) a septum and a cold trap for analyzing temperature programmed reactions. Also adds four gas inlets and a loop for performing pulse chemisorption analyses. Supplied with 500µl sample loop.
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Part No. 350-33631-CR OPTION - MKS Cirrus™2
Benchtop Atmospheric RGA System, 200AMU CR for 3Flex ECR 200 AMU mass spectrometer connects directly to a dedicated port on the 3Flex ECR for detection and identification of low concentrations of condensable and/or reactive gases. Enhanced Chemical Resistance (ECR) configuration.
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Part No. 350-33631-00 OPTION - MKS Cirrus™2
Benchtop Atmospheric RGA System, 200AMU CR for 3Flex 200 AMU mass spectrometer connects directly to a dedicated port on the 3Flex ECR for detection and identification of low
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Part No. 350-00001-CR 3Flex with 1 MP Port, ECR
Enhanced Chemical Resistance
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Part No. 350-00002-CR 3Flex with 2 MP Port, ECR
Enhanced Chemical Resistance
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Part No. 350-00003-CR 3Flex with 3 MP Port, ECR
Enhanced Chemical Resistance
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Part No. 350-00031-CR 3Flex Chemi with 1 MP Port, ECR
Enhanced Chemical Resistance
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Part No. 350-00032-CR 3Flex Chemi with 2 MP Port, ECR
Enhanced Chemical Resistance
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Part No. 350-00033-CR 3Flex Chemi with 3 MP Port, ECR
Enhanced Chemical Resistance
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Accessories

Cables

Part No. 003-63801-01 Cable
Ethernet straight-thru for connnecting instrument to control module (PC)
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Dewar dip stick

Part No. 240-25901-00 Dewar dip stick
Dip stick for checking liquid nitrogen lever in Dewar
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Dewar

Part No. 350-25853-04 Shield assembly
for dewar and chemisorption furnace
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Part No. 350-25825-00 Dewar assembly
3.2 ltr
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Dewar lids

Part No. 350-31700-00 Dewar lid 9mm
for 9mm sample tubes
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Part No. 350-31701-00 Dewar lid 12mm
for 12mm sample tubes
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Gas Regulator

Part No. 004-62230-32 Gas Regulator CO2
CGA 320, 30 psig, for use with CO2
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Part No. 004-62230-58 Gas regulator for He, N2, Kr, Ar
30 psig, CGA 580
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Gas Regulator Accessories

Part No. 004-25549-00 Reducer
1/8 in tube x 1/4 in tube
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Part No. 004-33601-00 Gas Regulator expansion kit
adds an additional outlet to the gas regulator
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Part No. 004-33602-00 Gas Regulator Pressure Relief Kit
prevents excessive gas pressure in the event of a regulator failure (not to be used with toxic gases)
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Part No. 004-25318-00 Reducer - for Chemisorption
1/4 stub × 1/8 tbg, SST
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Part No. 201-25818-00 Gas Inlet Line for Chemisorption
Gas Inlet Line, SS 6ft
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Gas Inlet Lines - copper

Part No. 290-25846-00 Gas Inlet Line copper 6'
Gas Inlet Line, 1/8 in x 6 ft long, copper
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Part No. 290-25846-01 Gas inlet line - copper
Gas Inlet Line, 1/8 in x 16 ft long, copper
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Isothermal Jacket

Part No. 350-25812-02 - Isothermal jacket
Isothermal Jacket, 9mm ID
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Part No. 350-25812-03 Isothermal Jacket
12mm ID
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Reference Material

Part No. 004-16844-00 Reference Material
Y Zeolite
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Part No. 004-16821-00 Reference material
Silica Alumina, ~ 215 m2/g, 10g
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Part No. 004-16825-00 Reference material
For Chemisorption - Reference Material, Platinum on alumina chemi
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Heating Mantle

Part No. 350-53700-00 Degas mantle
Top, Degas mantle top for 350-26000-00 (Glascol mantle)
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Part No. 350-26004-00 Mantle
Vapor Heating Mantle
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Part No. 350-53701-00 Mantle with top
Degas Mantle with top
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Part No. 350-53701-01 Degas Mantle top
for 350-53701-0
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Part No. 350-26012-00 Degas mantle
for use on instruments above serial number 200
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Vacuum Pump

Part No. 004-25509-00 Clamp
Clamp, NW 10/16
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Part No. 004-25626-04 Flex Tube
Flex Tube, 3/4 in OD × 48 in long, NW 16
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Part No. 004-25630-00 Centering Ring
NW 16
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Part No. 004-28998-02 Clamp, Hose
For Chemisorption Clamp, Hose, 7/32in - 5/8in
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Part No. 062-62803-00 Dry Diaphragm Vacuum Forepump
without tray
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Part No. 350-34006-00 Hybrid Pump
5×10-9 mbar
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Software and Manuals

Part No. 350-20800-00 software
3Flex - current version software
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Part No. 350-42800-00 operator manual
3Flex - operator’s manua
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Valves

Part No. 004-22601-06 Valve
Diaphragm Sealed Valve, 1/4 in male
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Part No. 004-62002-05 Valve
Solenoid Valve, 24 VDC, 2-way, without BASE
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Part No. 248-60802-36 Valve
Servo Valve cable, .030, SST
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Operating Supplies - Physisorption

Part No. 350-33609-00 Extended Operating Supplies, 9mm
Includes 9 sample tubes, 3 isothermal jackets, 1 service kit, reference materials, filler rods, O-rings and other accessories
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Part No. 350-33610-00 Extended Operating Supplies, 12mm
Includes: 9 sample tubes, 3 isothermal jackets, 1 service kit, reference materials, filler rods, O-rings and other accessories
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Sample Tubes and accessories

Part No. 004-25013-02 O-ring
-013 70 Duro Viton, Brown
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Part No. 004-25040-06 Gasket
1/2 in, SS, Retainer Assembly
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Part No. 004-25079-10 CHEMISORPTION O-RING
-009, VITON, BROWN
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Part No. 004-27070-00 Frit
20 µm, 1/4 in
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Part No. 004-32004-00 Rubber stopper
for sample tubes (fits various sample tube sizes)
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Part No. 004-54104-01 16" inch Brush
for cleaning sample tubes
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Part No. 004-54618-00 Tool
for removing the sample port O-ring
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Part No. 240-14855-00 Rack
sample tube holder
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Part No. 240-25853-00 Funnel
sample tube
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Part No. 300-32800-00 Support
sample weighing
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Part No. 350-25843-01 Ferrule
for 9 mm sample tube
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Part No. 350-61003-00 Hanging Filler Rod
for 9 mm sample tube
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Part No. 350-61002-02 Sample Tube
9 mm, flat bottom
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Part No. 350-25843-00 Ferrule
for 12 mm sample tube
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Part No. 350-25864-00 Check Seal assembly
for 12 mm sample tube
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Part No. 350-33608-00 TranSeal Kit

includes three TranSeals with alternate size O-rings. and installation instructions

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Part No. 350-61003-01 Hanging Filler Rod
for 12 mm sample tube
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Part No. 350-61002-03 Sample Tube
12 mm, flat bottom
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Part No. 350-61004-00 Filler
Check Seal
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Part No. 004-25040-05 Gasket
1/4in, SS, Retainer Assembly
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Part No. 004-25225-02 Ferrule
6mm, Rear, Stainless, For Chemisorption
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Part No. 240-32000-00 Stopper
For Chemisorption Stopper, for 1/2in OD tubes
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Part No. 248-32702-00 Filter Disc
For Chemisorption Filter Disc, Quartz (qty.100)
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Part No. 248-32702-00 Filter Disc
For Chemisorption, Quartz (qty.100)
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Part No. 350-25874-03 Nut
For Chemisorption, Sample Port, 6mm
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Part No. 350-25875-00 Assembly, Stand,
For Chemisorption, Sample Tube Weighing
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Part No. 350-33032-00
For Chemisorption Chemisorption Quartz Filter Discs Kit; includes quartz filter discs(packof100), quartz filter discs instructions, glass rod for filter disc installation
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Part No. 350-61003-02 Assembly Hanging Filler
For Chemisorption, Filler, Quartz
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Part No. 350-61030-00 For Chemisorption Tube
350-61030-00 Sample Flow thru, Quartz, 12mm
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Part No. 350-61032-00 Sample Flow-thru
For Chemisorption Tube, Quartz, 12mm, 6cc,bulb tube
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Part No. 350-61033-00 Glass rod
For Chemisorption, for filter disc installation
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Part No. 350-33603-00 Sample Tube Kit
12 mm; includes 9 O-rings, 9 stoppers, 3 isothermal jackets, 1 Dewar lid, 9 sample tubes, 3 hanging filler rods, 1 sample tube brush
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Part No. Part No. 350-33604-00 Sample Tube Kit
9 mm; includes 9 O-rings, 9 stoppers, 3 isothermal jackets, 9 ferrules, 1 Dewar lid, 9 sample tubes, 3 hanging filler rods, 1 sample tube brush
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Part No. 350-33607-00 Check Seal Kit
12 mm, includes 3 openers, 3 Check Seals, and 1 extractor tool
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FlowPrep 060

Part No. 060-00030-00 FlowPrep 060
degasses up to six samples at up to 400 ºC with flowing gas. A gas regulator is required.
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Part No. 060-00035-00 for 3Flex
FlowPrep 060
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VacPrep 061

VacPrep 061 for 3Flex, degasses up to six samples at up to 400 ºC; uses flowing gas or evacuation by vacuum. Evacuation requires a gas source and gas regulator 065-00035-00.
Part No. 061-00035-00 VacPrep 061
for 3Flex
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Pneumatic Filter Assembly

Part No. 350-34040-00 Pneumatic Filter Assembly
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Air Compressor

Part No. 011-62700-11 Air compressor
115 VAC 2.12 CFM, for operation of pneumatic valves
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Part No. 011-62700-23 Air compressor
230 VAC 2.12 CFM, for operation of pneumatic valves
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Part No. 350-34040-00 Pneumatic filter assembly
for air source
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Smart VacPrep

is an advanced six-port system that utilizes vacuum to prepare samples by heating and evacuation. Each of the ports may be operated independently. Samples may be added or removed from degas ports without disturbing the treatment of other samples undergoing preparation. Degassing automatically terminates when the samples have completed all programmed steps.
Part No. 067-00000-00 Smart VacPrep
without vacuum pump
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Part No. 067-00000-11 Smart VacPrep
110 volt
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Part No. 067-00000-22 Smart VacPrep
230 volt
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Part No. 067-00001-00 Smart VacPrep
with high-vacuum pump
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Gloves

For Chemisorption
Glove, Cotton Canvas, 8oz

Operating Supplies - Chemisorption

These supplies are for the 3Flex with Chemisorption option
Part No. 350-32802-00 Exhaust tube for instrument
1/4in. ID x 10 ft long. FOR CHEMISORPTION INSTRUMENT
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Part No. 004-25891-00 Clip
Sample Thermocouple for use with bulb sample tube. FOR CHEMISORPTION INSTRUMENT
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Part No. 350-33835-00 Cable
Sample Thermocouple, DB9, Type K FOR CHEMISORPTION INSTRUMEN
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Part No. 350-32801-00 Exhaust tube
for vacuum pump, 3/8in. ID x 10 ft long FOR CHEMISORPTION INSTRUMENT
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Part No. 350-33635-00 Chemisorption Extended Operating Supplies (6-month supply);
includes: O-rings, sample port dust frit, reference material, furnace insulator set, quartz hanging filler rod assembly, quartz wool, quartz filter discs, sample tube brush, sample tube stoppers, exhaust tubing. NOTE: Sample tubes are not included in the 3Flex Chemisorption Extended Operating Supplies. Sample tubes must be ordered separately.
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Part No. 350-33632-00 Chemisorption Extended Operating Supplies (12-month supply);
includes: O-rings, sample port dust frit, reference material, furnace insulator set, quartz hanging filler rod assembly, quartz wool, quartz filter discs, sample tube brush, sample tube stoppers, exhaust tubing. NOTE: Sample tubes are not included in the 3Flex Chemisorption Extended Operating Supplies. Sample tubes must be ordered separately.
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Part No. 350-31720-00 Furnace Insulator Set
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Sub-Ambient Temperature Control Devices

Part No. 350-33005-00, ISO Controller
Micromeritics’ ISO Controller utilizes thermoelectric cooling based on the Peltier principle. The unit is designed to maintain a constant temperature between 0 °C and 80 °C when using CO2, N2, and other gases for adsorption analysis. The device rapidly cools and efficiently maintains temperature with minimal electrical current required. The sample area will accommodate up to 3 sample tubes. Heat removal is uniform and accurate when the unit is used with an appropriate liquid (ambient water or liquid antifreeze). The dewar section is placed on the instrument dewar elevator and then raised into position for analysis.
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Part No. 025-00350-00, Chiller Dewar
Chiller Dewar - A closed plumbing system that circulates fluid from a temperature controlled bath into a small dewar filled with antifreeze in which the sample tubes are immersed.
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Part No. 025-26002-00, Recirculating Bath Recirculating Bath
-28 °C, to 200 °C, 230V 50Hz, Refrigerated and Heating Circulator for temperature control of the Chiller Dewar. Note: Recommended for use with the Chiller Dewar Option 025-00350-00
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Part No. 021-00000-00 Model 21 LN2 transfer system
or easy filling of sample Dewars; includes 47-L dewar, mobile platform, and pump with 100-cm discharge line
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Part No. 026-00350-00 Cryostat I
Single-Stage Cryogenic Refrigerator Based on the Gifford-McMahon Principle The Micromeritics Cryostat I is a closed-cycle cryocooler based on the Gifford-McMahon (GM) refrigeration principle. It uses helium gas from a helium compressor to generate cryogenic temperatures. The refrigeration effect of the GM cooler results from a series of thermodynamic processes acting on the helium gas that includes: charging and compression, displacement and heat exchange with the regenerator, expansion and heat absorption (cooling effect).
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