PARTICLE SIZE AND PARTICLE SHAPE

Laser Light Scattering – Mie and Fraunhofer Theories

PSA – 01 (Formerly 520-00)

Aqueous – dispersion (ISO 13320) using Saturn DigiSizer

USA only

PSA – 02 (Formerly 520-01)

Non-aqueous – based dispersion (ISO 13320) using Saturn DigiSizer

USA only

PSA – 03 (Formerly 520-50)

Dry dispersion (ISO 13320) using Malvern Mastersizer

USA only

PSA – 04 (Formerly 520-51)

Liquid dispersion (ISO 13320) using Malvern Mastersizer

USA only

X – Ray Sedimentation – Stokes’ Law

PSA- 05 (Formerly 510-00)

Aqueous and non-aqueous based dispersion inorganic materials only (ISO 13317-3) (Requires Density- 01 prior to analysis if skeletal density is not provided

280€

Particle Shape Analysis

PSA-13 (Formerly 005-80)

Particle shape using wet dispersion and dynamic image analysis (ISO 13322-2)

USA only

SEM – 04 (Formerly 005-81)

Particle shape using an automated microscopy technique

USA only

Nano Particle Size

Physi – 23 (Formerly 005-70)

Average particle size calculated from BET surface area

280€

PSA-10 (Formerly 005-71)

Dynamic light scattering/ photon correlation spectroscopy (ISO 22412)

USA only

Other Particle Size Techniques

PSA-11 (Formerly 005-73)

Particulate count and concentration using the light obscuration technique (USP method <788> and<789>)

USA only

PSA-12 (Formerly 005-74)

Sub-Sieve AutoSizer (ASTM B330-07 , ASTM C721, 150-10070) (Requires density prior to analysis) Air permeability diameter

USA only

PSA-14 (Formerly 010-16)

Dry or wet sieving available/ Ro-Tap apparatus

USA only

PSA-15 (Formerly 010-78)

Particle size of material on filters

USA only

SEM – 03 (Formerly 010-SO)

Particle size using automated microscopy techniques

USA only

Zeta Potential

PSA-16 (Formerly 120 -00)

Zeta potential (ISO 13099-2)

USA only

PSA-17 (Formerly 120-01)

ISO-electric point determination and pH titration

USA only

Mayer – Stowe

PSA-18 (Formerly 942 -09)

Particle size calculation from Mercury intrusion analysis

340€

B.E.T. OR LANGMUIR SURFACE AREA; T-PLOT AREA

Physi – 01 (Formerly 005-01)

Multipoint surface area using nitrogen gas (ISO 9277)

230€

Physi – 02 (Formerly 005-02)

Multipoint surface area using krypton gas (ISO 9277)

260€

Physi – 04 (Formerly 005-10)

Multipoint surface area and STSA using nitrogen gas (ASTM D6556)

310€

PORE VOLUME DISTRIBUTION/PORE SIZE DISTRIBUTION

Pore Size by Gas Adsorption:

Pore size samples may include the following reports as appropriate: BET or Langmuir surface area, BJH mesopore analysis, DFT pore size calculations, single-point total pore volume, and t-Plot micropore volume (ISO 15901-02).

Physi – 10 (Formerly 005-50)

40-point nitrogen adsorption isotherm (20 A to 3000 A)

370€

Physi -12 (Formerly 005-08)

40-pt Nitrogen adsorption and 40-pt desorption isotherm (20 A to 3000 A)

530€

Micropore Pore Size Distribution:

Reports may include H-K, Dubinin, and/or DFT methods for micropore analysis (ISO 15901-3) .

Physi-13 (Formerly 201-03)

High-resolution micropore analysis plus mesopore isotherm (4 A to 3000 A)

930€

Pore Size by Mercury Intrusion

Report will include calculations of bulk density, skeletal density, porosity, average pore diameters, median pore diameters, and total intrusion volume. Additional summary reports such as tortuo slty, fractal dimension, permeability, and compressibility are available upon request for an additional fee (ISO 15901-01).

MIP – 01 (Formerly 942-03)

Mercury intrusion analysis (pore size range 360 to 0.003 μm)

345€

MIP – 02 (Formerly 942 – 04)

Mercury Intrusion and extrusion analysis (pore size range 360 to 0.003 μm)

390€

MIP -03 (Formerly 942-10)

High-resolution macropore analysis (pore size range 900 to 4 μm)

320€

MIP – 04 (Formerly 942 -11)

High-resolution macropore plus a complete intrusion and extrusion analysis

490€

MIP-05

Reverberi method for pore throat and pore cavity

585€

MIP – 10 (Formerly 942-05)

Advanced Hg calculations

75€

DENSITY

Density- 01 (Formerly 133 – 00)

Skeletal density (Helium or Nitrogen pycnometry) ISO 12154, USP <699>

125€

Density- 02 (Formerly 133 – 01)

Skeletal density at specific temperature

150€

Density – 03 (Formerly 133 – 02)

Open cell content of rigid cellular plastic, foam density (ASTM 06226)

200€

Density- 04 (Formerly 136 – 00)

Envelope density of solid, non-powder samples using the GeoPyc”‘ 1360

150€

Density- 05 (Formerly 136 – 01)

T.A.P.™ (Transverse Axial Pressure) density using the GeoPyc® 1360

200€

Density – 07 (Formerly 942 – 07)

Mercury bulk density

265€

Density – 08 (Formerly 010 – 70)

Bulk and Tap density USP <616>

175€

Density – 09 (Formerly 010 – 77)

Bulk density only

125€

SPECIAL VAPOR SORPTION SERVICES

Physi – 20 (Formerly 005 – 60)

Special CO2 isotherms at O °C

565€

Physi – 21 (Formerly 005 – 60)

Adsorption isotherms at user defined conditions (specialty gases)

875€

Physi – 22 (Formerly 005 – 61)

High-pressure isotherms using hydrogen, nitrogen, oxygen, methane, or other gases

USA only

Vapor – 01 (Formerly 005 – 63)

Vapor isotherms – Dynamic vapor sorption (DVS) gravimetric analysis

USA only

Vapor – 02 (Formerly 005 – 64)

Vapor isotherms using volumetric technique (ASAP 2020 or 3Flex)

775€

Vapor – 03 (Formerly 005 – 65)

Inverse gas chromatography (surface energy measurement)

USA only

Vapor- 04 (Formerly 005 – 75)

Surface energy heterogeneity profile (BET surface area required)

USA only

CHEMISORPTION

Chemi – 01 (Formerly 201 -10)

Volumetric chemisorption analysis (specify analytical method)

USA only

Chemi – 02 (Formerly 291- 23)

Dynamic or pulse chemisorption analysis (specify analytical method)

730€

Chemi – 03 (Formerly 291- 03)

Pulse chemisorption using liquid vapors (specify analytical method)

820€

Temperature-Programmed Studies

Chemi – 04 (Formerly 291- 01)

Temperature-Programmed Reduction (TPR)

620€

Chemi – 05 (Formerly 291-10)

Temperature-Programmed Desorption (TPD)

620€

Chemi – 06 (Formerly 291- 02)

Temperature-Programmed Oxidation (TPO)

620€

Chemi – 07 (Formerly 291- 06)

Mass spectrometry analysis (must be combined with temperature program study)

USA only

Other Chemisorption Experiments

Chemi – 20 (Formerly 005 – 62)

High-pressure reactions using AutoChem 2950

USA only

Chemi – 21 (Formerly 201- SO)

Isosteric heat of adsorption

1240€

Chemi – 22 (Formerly 291- 20)

Heat of desorption, first order kinetics

1750€

MICROSCOPY

SEM – 01 (Formerly 010 – 40)

SEM images using table-top SEM

USA only

SEM – 02 (Formerly 010 – 41)

Elemental analysis by energy dispersion spectroscopy and SEM Imaging

USA only

SEM – 05 (Formerly 010- 23)

Images from optical microscope

USA only

THERMAL ANALYSIS

Thermal – 01 (Formerly 005 – 66)

TGA- Standard run conditions room temp – 900°C

USA only

Thermal – 02 (Formerly 005 – 67)

DSC- Standard run room temp – 600°C

USA only

Thermal – 03 (Formerly 005 – 68)

mDSC – Modulated DSC- High resolution

USA only

Thermal – 04 (Formerly 005 – 69)

Combination TGA/DSC

USA only

POWDER RHEOLOGY

Powder – 01

Complete set of powder testing using the FT4, including dynamic flow properties, bulk powder properties and shear properties. A summary report will be provided.

USA only

Powder – 02

Dynamic flow properties Include basic flowability , aeration test ing and consolidation test ing along with summary report.

USA only

Powder – 03

Bulk powder property testing includes compressibility and permeability testing along with a summary report

USA only

Powder- 04

Shear property testing includes shear cell testing and wall friction testing along with a summary report.

USA only

Powder-05

Individual powder property testing , choose from flowability , aeration, consolidation, compressibility, permeability, shear and wall friction testing. Price Is per test and per sample. No summary report available.

USA only

CAPILLARY FLOW POROMETRY

Filter-01

Scanning porometry of pore sizes down to 30 nm using a POROLUXTM 100/l OONW; 500

USA only

SCIENTIFIC SERVICES

PTA- 01 (Formerly 010 – 00)

Non-standard laboratory analysis

Call

PTA-02 (Formerly 010-10)

Method development services

Call

PTA- 03 (Formerly 010-11)

Method validation services

Call

PTA-04

Method verification or method transfer

Call

PTA- 05 (Formerly 010- 06)

Consulting services and detailed results interpretation

Call

OTHER SERVICES

PTA-06 (Formerly 010-80)

Special sample preparation or storage (glove box or freezer)

USA only

PTA – 10 ( Formerly 005 – 87)

Expert testimony

Call

PTA-13 (Formerly 010-01)

Certificate of analysis

75€

PTA-40 (Formerly 005- 85)

Dynamic void volume – DVVA (ASTM D7854)

USA only

PTA-41 (Formerly 005-86)

Magnetic content using Buck MA-1040 Analyzer

USA only

PTA- 42 (Formerly 010-15)

Viscosity of liquids using cone/plate rheometer

USA only

SEM – 03 (Formerly 010 – 50) Call

Contamination or particle identification (outsourced)

Call

MIP-11 (Formerly 950-50)

Volume calibration of AutoPore Mercury penetrometers

260€

VOLUME DISCOUNT SCHEDULE

Volume discounts are based on the number of samples sent in for same test number, not just total number of samples .

6-10 samples

5% Discount

11-20 samples

10% Discount

21-40 samples

15% Discount

More than 40 samples

20% Dicount

SAMPLE TURNAROUND TIMES

Turnaround times are typical for most samples. Some exclusions do apply.

Normal (Typically within 7 business days)

List Price

Priority (Typically2 to 4 business days)

List Price + 50% surcharge

Rush (Next sample analyzed)

List Price+ 200% surcharge

All orders are subject to Particle Testing Authority terms and conditions (see separate terms and conditions document at www.particletesting.com ). Credit card orders are welcomed .
Unless otherwise requested, samples will be retained for a minimum of 3 months. Samples can be returned at the customer’s expense, provided correct shipping and payment information is received. Sample results will be maintained for a minimum of 5 years. All samples and related customer information is kept confidential.

INSTRUMENT PURCHASE ALLOWANCE

Half the cost of applicable analyses completed within 120 days of instrument purchase may be credited toward instrument purchase. The maximum credit allowed is 4% of the instrument purchase price. Customer must notify Micromeritics of credit due when instrument is ordered.

RETURN SAMPLE FEE

There is a flat fee of 60€ per project for all sample returns. 160€ if samples are considered hazardous. unless an account number is provided. SDS are required for all samples .

Please review the Terms and Conditions

TERMS: Net 30 days … for 45 days add 2%, for 60 days add 4% to the final negotiated price .

 

For tests available in USA only, please see USA price list and contact the Norcross, GA Laboratory at [email protected]